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Colin Fyfe

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Research and Teaching Interests

Dr. Fyfe's general area of interest is in the application of NMR spectroscopy to the investigation and characterization of solids of chemical interest and includes the synthesis of a wide variety of materials and construction of appropriate hardware and the use of complementary techniques such as X-ray diffraction and electron microscopy. Current efforts emphasize high resolution solid-state NMR techniques and NMR microimaging.

In contrast to NMR spectra of liquids and solutions where very narrow signals are observed which can be used for structure elucidations, the NMR spectra of solids generally exhibit broad, mainly featureless absorptions. It is now possible to obtain the same "isotropic average" spectra in the solid state by a combination of the techniques of magnetic dilution, dipolar decoupling and &quo t;Magic Angle" spinning and to increase the signal/noise by cross-polarization. These spectra may be used to determine the structures of solid materials, even if they are non-crystalline, and a large range of nuclei such as 13C, 29Si, 27Al, 11B, 31P can be easily observed. Using these techniques we are investigating a wide variety of solids including polymers, catalysts, gels, surfaces, zeolites and organic and organometallic solids.

In NMR imaging, the three-dimensional distribution of a liquid within a solid matrix may be determined in a non-invasive and nondestructive manner (It should be emphasized that only the mobile component is imaged). Current work is centered on multinuclear imaging of small samples with as high a resolution as possible and investigating the effect of temperature on tissue treated with cryoprotectants and the interaction of polymers and composites with liquids and gases.

                                             Lattice structure of zeolite ZSM-5 (Mobil Corp.)

Lattice structure of zeolite ZSM-5 (Mobil Corp.), the "wonder catalyst" which converts methanol to gasoline together with its high-resolution 29Si MAS NMR spectrum. Changes in the spectra as a function of temperature and when organic molecules are added indicate that the lattice structure changes to accommodate the guest organics.

Fyfe Group - Richard zeolite

 

Fyfe Group

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Real name: 
Colin Fyfe
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Curriculum Vitae

B.Sc., St. Andrews (1964); Ph.D., St. Andrews (R. Foster, 1966); Medical Research Council Fellow, St. Andrews (1966-67); Killam Postdoctoral Fellow, U.B.C. (C.A. McDowell, 1967-69); Assistant Professor, Guelph (1969-72); Associate Professor, Guelph (1972-78); Professor, Guelph (1978-87); Merck, Sharp and Dohme Award (1981); Sigma Xi Award (1984); Canada Council Killam Research Fellow (1985-87); Barringer Award of Canadian Spectroscopy Society (1985); Fellow of the Royal Society of Canada (1986); Senior Killam Award (1991).

Publications

2008

Fyfe, C. A. ; Lee, J. S. J. Solid-State Nmr Determination Of The Zeolite Zsm-5/ortho-Xylene Host-Guest Crystal Structure. Journal of Physical Chemistry C 2008, 112, 500-513.
Fyfe, C. A. ; Darton, R. J. ; Schneider, C. ; Scheffler, F. Solid-State Nmr Investigation Of The Possible Existence Of "nanoblocks" In The Clear Solution Synthesis Of Mfi Materials. Journal of Physical Chemistry C 2008, 112, 80-88.
Fyfe, C. A. ; Lee, J. S. J. ; Cranswick, L. M. D. ; Swainson, I. Powder Neutron Diffraction Determination Of The Structure Of The O-Xylene/zeolite Zsm-5 Complex. Microporous and Mesoporous Materials 2008, 112, 299-307.

2007

Li, F. ; Wang, Z. Y. ; Ergang, N. S. ; Fyfe, C. A. ; Stein, A. Controlling The Shape And Alignment Of Mesopores By Confinement In Colloidal Crystals: Designer Pathways To Silica Monoliths With Hierarchical Porosity. Langmuir 2007, 23, 3996-4004.
Kasai, M. ; Lewis, A. R. ; Ayabe, S. ; Hatae, K. ; Fyfe, C. A. Quantitative Nmr Imaging Study Of The Cooking Of Japonica And Indica Rice. Food Research International 2007, 40, 1020-1029.

2006

Fyfe, C. A. ; Brouwer, D. H. Optimization, Standardization, And Testing Of A New Nmr Method For The Determination Of Zeolite Host-Organic Guest Crystal Structures. Journal of the American Chemical Society 2006, 128, 11860-11871.
Brouwer, D. H. ; Chezeau, J. M. ; Fyfe, C. A. Solid State Nmr Investigation Of The Structure Of Alpo4-14A. Microporous and Mesoporous Materials 2006, 88, 163-169.
Fyfe, C. A. ; Brouwer, D. H. Determination Of The Location Of Naphthalene In The Zeolite Zsm-5 Host Framework By Solid-State H-1/si-29 Cp Mas Nmr Spectroscopy. Canadian Journal of Chemistry-Revue Canadienne De Chimie 2006, 84, 345-355.

2005

Fyfe, C. A. ; Diaz, A. C. ; Grondey, H. ; Lewis, A. R. ; Forster, H. Solid State Nmr Method For The Determination Of 3D Zeolite Framework/sorbate Structures: H-1/si-29 Cp Mas Nmr Study Of The High-Loaded Form Of P-Xylene In Zsm-5 And Determination Of The Unknown Structure Of The Low-Loaded Form. Journal of the American Chemical Society 2005, 127, 7543-7558.
Fyfe, C. A. ; Brouwer, D. H. ; Tekely, P. Measurement Of Nmr Cross-Polarization (Cp) Rate Constants In The Slow Cp Regime: Relevance To Structure Determinations Of Zeolite-Sorbate And Other Complexes By Cp Magic-Angle Spinning Nmr. Journal of Physical Chemistry A 2005, 109, 6187-6192.
Brouwer, D. H. ; Kristiansen, P. E. ; Fyfe, C. A. ; Levitt, M. H. Symmetry-Based Si-29 Dipolar Recoupling Magic Angle Spinning Nmr Spectroscopy: A New Method For Investigating Three-Dimensional Structures Of Zeolite Frameworks. Journal of the American Chemical Society 2005, 127, 542-543.
Gardiennet, C. ; Marica, F. ; Fyfe, C. A. ; Tekely, P. Determining The Geometry Of Strongly Hydrogen-Bonded Silanols In A Layered Hydrous Silicate By Solid-State Nuclear Magnetic Resonance. Journal of Chemical Physics 2005, 122, 10.
Gardiennet, C. ; Marica, F. ; Fyfe, C. A. ; Tekely, P. Determining The Geometry Of Strongly Hydrogen-Bonded Silanols In A Layered Hydrous Silicate By Solid-State Nuclear Magnetic Resonance (Vol 122, Pg 054705, 2005). Journal of Chemical Physics 2005, 122, 1.
Kasai, M. ; Lewis, A. ; Marica, F. ; Ayabe, S. ; Hatae, K. ; Fyfe, C. A. Nmr Imaging Investigation Of Rice Cooking. Food Research International 2005, 38, 403-410.

2004

Darton, R. J. ; Brouwer, D. H. ; Fyfe, C. A. ; Villaescusa, L. A. ; Morris, R. E. Measuring The Silion Fluoride Bond Distance In Zeolites. In Recent Advances in the Science and Technology of Zeolites and Related Materials, Pts a - C; VanSteen, E. ; Claeys, M. ; Callanan, L. H. ; Recent Advances in the Science and Technology of Zeolites and Related Materials, Pts a - C; Elsevier Science Bv: Amsterdam, 2004; Vol. 154, pp. 1319-1323.
Fyfe, C. A. ; Bretherton, J. L. ; Skibsted, J. ; Zahedi-Niaki, M. H. ; Kalliaguine, S. Solid State Nmr Studies Of The Hydration Of Molecular Sieve Alpo-36. In Recent Advances in the Science and Technology of Zeolites and Related Materials, Pts a - C; VanSteen, E. ; Claeys, M. ; Callanan, L. H. ; Recent Advances in the Science and Technology of Zeolites and Related Materials, Pts a - C; Elsevier Science Bv: Amsterdam, 2004; Vol. 154, pp. 1238-1245.
Moorlag, C. ; Yang, Q. Z. ; Troczynski, T. ; Bretherton, J. ; Fyfe, C. Aluminum Phosphates Derived From Alumina And Alumina-Sol-Gel Systems. Journal of the American Ceramic Society 2004, 87, 2064-2071.
Do, T. O. ; Nossov, A. ; Springuel-Huet, M. A. ; Schneider, C. ; Bretherton, J. L. ; Fyfe, C. A. ; Kaliaguine, S. Zeolite Nanoclusters Coated Onto The Mesopore Walls Of Sba-15. Journal of the American Chemical Society 2004, 126, 14324-14325.
Fyfe, C. A. ; Brouwer, D. H. Effect Of Molecular Oxygen On The Variable-Temperature Si-29 Mas Nmr Spectra Of Zeolite-Sorbate Complexes. Journal of the American Chemical Society 2004, 126, 1306-1307.
Darton, R. J. ; Brouwer, D. H. ; Fyfe, C. A. ; Villaescusa, L. A. ; Morris, R. E. Solid-State Nmr Studies Of The Fluoride-Containing Zeolite Ssz-44. Chemistry of Materials 2004, 16, 600-603.

2003

Fechtelkord, M. ; Behrens, H. ; Holtz, F. ; Bretherton, J. L. ; Fyfe, C. A. ; Groat, L. A. ; Raudsepp, M. Influence Of F Content On The Composition Of Al-Rich Synthetic Phlogopite: Part Ii. Probing The Structural Arrangement Of Aluminum In Tetrahedral And Octahedral Layers By Al-27 Mqmas And H-1/f-19-Al-27 Hetcor And Redor Experiments. American Mineralogist 2003, 88, 1046-1054.
Groat, L. A. ; Chakoumakos, B. C. ; Brouwer, D. H. ; Hoffman, C. M. ; Fyfe, C. A. ; Morell, H. ; Schultz, A. J. The Amblygonite (Lialpo4F)-Montebrasite (Lialpo4Oh) Solid Solution: A Combined Powder And Single-Crystal Neutron Diffraction And Solid-State Li-6 Mas, Cp Mas, And Redor Nmr Study. American Mineralogist 2003, 88, 195-210.
Fechtelkord, M. ; Behrens, H. ; Holtz, F. ; Fyfe, C. A. ; Groat, L. A. ; Raudsepp, M. Influence Of F Content On The Composition Of Al-Rich Synthetic Phlogopite: Part 1. New Information On Structure And Phase-Formation From Si-29, H-1, And F-19 Mas Nmr Spectroscopies. American Mineralogist 2003, 88, 47-53.

2002

Morell, H. ; Angermund, K. ; Lewis, A. R. ; Brouwer, D. H. ; Fyfe, C. A. ; Gies, H. Structural Investigation Of Silicalite-I Loaded With N-Hexane By X-Ray Diffraction, Si-29 Mas Nmr, And Molecular Modeling. Chemistry of Materials 2002, 14, 2192-2198.
Fyfe, C. A. ; Diaz, A. C. Investigation Of Slow Molecular Motions And Chemical Exchange In The High Loaded Form Of P-Xylene In Zsm-5 By Two-Dimensional C-13 Solid-State Nmr Exchange Experiments. Journal of Physical Chemistry B 2002, 106, 2261-2268.
Fyfe, C. A. ; Brouwer, D. H. ; Lewis, A. R. ; Villaescusa, L. A. ; Morris, R. E. Combined Solid State Nmr And X-Ray Diffraction Investigation Of The Local Structure Of The Five-Coordinate Silicon In Fluoride-Containing As-Synthesized Stf Zeolite. Journal of the American Chemical Society 2002, 124, 7770-7778.
McLean, B. W. ; Boraston, A. B. ; Brouwer, D. ; Sanaie, N. ; Fyfe, C. A. ; Warren, R. A. J. ; Kilburn, D. G. ; Haynes, C. A. Carbohydrate-Binding Modules Recognize Fine Substructures Of Cellulose. Journal of Biological Chemistry 2002, 277, 50245-50254.

2001

Fyfe, C. A. ; Skibsted, J. ; Schwieger, W. Solid-State Nmr Characterization Of The Mineral Searlesite And Its Detection In Complex Synthesis Mixtures. Inorganic Chemistry 2001, 40, 5906-5912.
Daniels, P. ; Fyfe, C. A. Al,si Order In The Crystal Structure Of Alpha-Eucryptite (Lialsio4). American Mineralogist 2001, 86, 279-283.
Fyfe, C. A. ; Bretherton, J. L. ; Lam, L. Y. Solid-State Nmr Detection, Characterization, And Quantification Of The Multiple Aluminum Environments In Us-Y Catalysts By Al-27 Mas And Mqmas Experiments At Very High Field. Journal of the American Chemical Society 2001, 123, 5285-5291.
Fechtelkord, M. ; Posnatzki, B. ; Buhl, J. C. ; Fyfe, C. A. ; Groat, L. A. ; Raudsepp, M. Characterization Of Synthetic Cs-Li Cancrinite Grown In A Butanediol-Water System: An Nmr Spectroscopic And Rietveld Refinement Study. American Mineralogist 2001, 86, 881-888.
Fyfe, C. A. ; Brouwer, D. H. ; Lewis, A. R. ; Chezeau, J. M. Location Of The Fluoride Ion In Tetrapropylammonium Fluoride Silicalite-1 Determined By H-1/f-19/si-29 Triple Resonance Cp, Redor, And Tedor Nmr Experiments. Journal of the American Chemical Society 2001, 123, 6882-6891.

2000

Tansho, M. ; Fyfe, C. A. ; Grondey, H. ; Markus, T. ; Wada, H. First Observation Of A Residual Inter-Cationic Correlation In The ’Super’-Ionic Conductor, Ag9Gase6: Ag-109-Ag-107 Double-Resonance Nmr Study Of Ion Dynamics. Solid State Ionics 2000, 132, 87-92.
Fyfe, C. A. ; Grondey, H. ; Blazek-Welsh, A. I. ; Chopra, S. K. ; Fahie, B. J. Nmr Imaging Investigations Of Drug Delivery Devices Using A Flow-Through Usp Dissolution Apparatus. Journal of Controlled Release 2000, 68, 73-83.
Fyfe, C. A. ; Lewis, A. R. Investigation Of The Viability Of Solid-State Nmr Distance Determinations In Multiple Spin Systems Of Unknown Structure. Journal of Physical Chemistry B 2000, 104, 48-55.
Hochgrafe, M. ; Gies, H. ; Fyfe, C. A. ; Feng, Y. ; Grondey, H. Lattice Energy-Minimization Calculation In The Further Investigation Of Xrd And Nmr Studies Of Zeolite Frameworks. Chemistry of Materials 2000, 12, 336-342.
Fyfe, C. A. ; Bretherton, J. L. ; Lam, L. Y. Detection Of The ’Invisible Aluminium’ And Characterisation Of The Multiple Aluminium Environments In Zeolite Usy By High-Field Solid-State Nmr. Chemical Communications 2000, 1575-1576.
Fyfe, C. A. ; Blazek-Welsh, A. I. Quantitative Nmr Imaging Study Of The Mechanism Of Drug Release From Swelling Hydroxypropylmethylcellulose Tablets. Journal of Controlled Release 2000, 68, 313-333.
Fyfe, C. A. ; Brouwer, D. H. Solid-State Nmr And X-Ray Diffraction Structural Investigations Of The P-Nitroaniline/zsm-5 Complex. Microporous and Mesoporous Materials 2000, 39, 291-305.

1999

Fyfe, C. A. ; Lewis, A. R. ; Chezeau, J. M. A Comparison Of Nmr Distance Determinations In The Solid State By Cross Polarization, Redor, And Tedor Techniques. Canadian Journal of Chemistry-Revue Canadienne De Chimie 1999, 77, 1984-1993.
Wolf, I. ; Gies, H. ; Fyfe, C. A. Ordering Of Silicate Layers By Hydrogen-Bonding Networks: Solid State Nmr Investigation Of The Perfect Three-Dimensional Registration In The Layer Silicate Rub-18. Journal of Physical Chemistry B 1999, 103, 5933-5938.
Fyfe, C. A. ; Altenschildesche, H. M. Z. ; Skibsted, J. Characterization Of Na5P3O10 Polymorphs By Na-23 Mas, Na-23 Mqmas, And P-31 Mas Nmr Spectroscopy. Inorganic Chemistry 1999, 38, 84-92.
Zahedi-Niaki, M. H. ; Xu, G. Y. ; Meyer, H. ; Fyfe, C. A. ; Kaliaguine, S. Synthesis And Characterization Of Alpo4-36: A Novel Aluminophosphate Molecular Sieve With Ats Structure. Microporous and Mesoporous Materials 1999, 32, 241-250.

1998

Schwieger, W. ; Altenschildesche, H. M. Z. ; Kokotailo, G. T. ; Fyfe, C. A. Low Temperature Syntheses Of Highly-Ordered Framework Materials: The Aluminium Phosphate Ammonium Taranakite. Zeitschrift Fur Anorganische Und Allgemeine Chemie 1998, 624, 1712-1717.
Preston, C. M. ; Trofymow, J. A. ; Niu, J. ; Fyfe, C. A. (13)Cpmas-Nmr Spectroscopy And Chemical Analysis Of Coarse Woody Debris In Coastal Forests Of Vancouver Island. Forest Ecology and Management 1998, 111, 51-68.
Fyfe, C. A. ; Blazek, A. I. Complications In Investigations Of The Swelling Of Hydrogel Matrices Due To The Presence Of Trapped Gas. Journal of Controlled Release 1998, 52, 221-225.
Gies, H. ; Marler, B. ; Vortmann, S. ; Oberhagemann, U. ; Bayat, P. ; Krink, K. ; Rius, J. ; Wolf, I. ; Fyfe, C. New Structures - New Insights: Progress In Structure Analysis Of Nanoporous Materials. Microporous and Mesoporous Materials 1998, 21, 183-197.
Fahie, B. J. ; Nangia, A. ; Chopra, S. K. ; Fyfe, C. A. ; Grondey, H. ; Blazek, A. Use Of Nmr Imaging In The Optimization Of A Compression-Coated Regulated Release System. Journal of Controlled Release 1998, 51, 179-184.

1997

Fyfe, C. A. ; Altenschildesche, H. M. Z. ; Wong-Moon, K. C. ; Grondey, H. ; Chezeau, J. M. 1D And 2D Solid State Nmr Investigations Of The Framework Structure Of As-Synthesized Alpo4-14. Solid State Nuclear Magnetic Resonance 1997, 9, 97-106.
Fyfe, C. A. ; Lewis, A. R. ; Chezeau, J. M. ; Grondey, H. F-19/si-29 Distance Determinations In Fluoride-Containing Octadecasil From Solid-State Nmr Measurements. Journal of the American Chemical Society 1997, 119, 12210-12222.
Fyfe, C. A. ; Skibsted, J. ; Grondey, H. ; Altenschildesche, H. M. zu Pulsed Field Gradient Multiple-Quantum Mas Nmr Spectroscopy Of Half-Integer Spin Quadrupolar Nuclei. Chemical Physics Letters 1997, 281, 44-48.
Isbell, S. A. ; Fyfe, C. A. ; Ammons, R. L. M. ; Pearson, B. Measurement Of Cryoprotective Solvent Penetration Into Intact Organ Tissues Using High-Field Nmr Microimaging. Cryobiology 1997, 35, 165-172.
Fyfe, C. A. ; Blazek, A. I. Investigation Of Hydrogel Formation From Hydroxypropylmethylcellulose (Hpmc) By Nmr Spectroscopy And Nmr Imaging Techniques. Macromolecules 1997, 30, 6230-6237.
Fyfe, C. A. ; Aroca, P. P. A Kinetic Analysis Of The Initial Stages Of The Sol-Gel Reactions Of Methyltriethoxysilane (Mtes) And A Mixed Mtes/tetraethoxysilane System By High-Resolution Si-29 Nmr Spectroscopy. Journal of Physical Chemistry B 1997, 101, 9504-9509.

1996

Fyfe, C. A. ; Wongmoon, K. C. ; Huang, Y. Al-27/p-31 Solid-State Nmr Structural Investigations Of Alpo4-5 Molecular Sieve. Zeolites 1996, 16, 50-55.
Fyfe, C. A. ; Mel, Z. ; Grondey, H. Investigation Of Fluorocarbon Blowing Agents In Insulating Polymer Foams By F-19 Nmr Imaging. Magnetic Resonance Imaging 1996, 14, 887-889.
Hochgrafe, M. ; Marler, B. ; Gies, H. ; Fyfe, C. A. ; Feng, Y. ; Grondey, H. ; Kokotailo, G. T. The Structure Of The Low Temperature (20 K) Form Of Zeolite Zsm-11 Derived From Si-29 Mas Nmr Spectroscopy, Lattice Energy Minimization And Rietveld Refinement. Zeitschrift Fur Kristallographie 1996, 211, 221-227.

1995

Kokotailo, G. T. ; Fyfe, C. A. ; Feng, Y. ; Grondey, H. ; Gies, H. ; Marler, B. ; Cox, D. E. Powder X-Ray Diffraction And Solid State Nmr Techniques For Zeolite Structure Determination. In Catalysis by Microporous Materials; Beyer, H. K. ; Karge, H. G. ; Kiricsi, I. ; Nagy, J. B. ; Catalysis by Microporous Materials; Elsevier Science Publ B V: Amsterdam, 1995; Vol. 94, pp. 78-100.
Fyfe, C. A. ; Fu, G. Y. Structure Organization Of Silicate Polyanions With Surfactants - A New Approach To The Syntheses, Structure Transformations, And Formation Mechanisms Of Mesostructural Materials. Journal of the American Chemical Society 1995, 117, 9709-9714.
Fyfe, C. A. ; Wongmoon, K. C. ; Huang, Y. ; Grondey, H. Inept Experiments In Solid-State Nmr. Journal of the American Chemical Society 1995, 117, 10397-10398.
Fyfe, C. A. ; Aroca, P. P. Quantitative Kinetic-Analysis By High-Resolution Si-29 Nmr-Spectroscopy Of The Initial-Stages In The Sol-Gel Formation Of Silica-Gel From Tetraethoxysilane. Chemistry of Materials 1995, 7, 1800-1806.
Fyfe, C. A. ; Wongmoon, K. C. ; Huang, Y. ; Grondey, H. Structural Investigations Of Sapo-37 Molecular-Sieve By Coherence-Transfer And Dipolar-Dephasing Solid-State Nuclear-Magnetic-Resonance Experiments. Microporous Materials 1995, 5, 29-37.
Fyfe, C. A. ; Wongmoon, K. C. ; Huang, Y. ; Grondey, H. ; Mueller, K. T. Dipolar-Based Al-27-]Si-29 Solid-State Nmr Connectivity Experiments In Zeolite Molecular-Sieve Frameworks. Journal of Physical Chemistry 1995, 99, 8707-8716.
Fyfe, C. A. ; Niu, J. Direct Solid-State C-13 Nmr Evidence For Covalent Bond Formation Between An Immobilized Vinylsilane Linking Agent And Polymer Matrices. Macromolecules 1995, 28, 3894-3897.
Fyfe, C. A. ; Niu, J. ; Mok, K. Synthesis And Characterization Of Polyfunctional Cross-Linking Agents For Cyanate Resins. Journal of Polymer Science Part a-Polymer Chemistry 1995, 33, 1191-1202.
Fu, G. Y. ; Fyfe, C. A. ; Schwieger, W. ; Kokotailo, G. T. Structure Organization Of Aluminosilicate Polyanions With Surfactants - Optimization Of Al Incorporation In Aluminosilicate Mesostructural Materials. Angewandte Chemie-International Edition 1995, 34, 1499-1502.
Schwieger, W. ; Pohl, K. ; Brenn, U. ; Fyfe, C. A. ; Grondey, H. ; Fu, G. ; Kokotailo, G. T. Isomorphous Substitution Of Silicon By Boron Or Aluminum In Layered Silicates. In Catalysis by Microporous Materials; Beyer, H. K. ; Karge, H. G. ; Kiricsi, I. ; Nagy, J. B. ; Catalysis by Microporous Materials; Elsevier Science Publ B V: Amsterdam, 1995; Vol. 94, pp. 47-54.
Fyfe, C. A. ; Grondey, H. ; Diaz, A. C. ; Kokotailo, G. T. ; Feng, Y. ; Huang, Y. ; Wongmoon, K. C. ; Mueller, K. T. ; Strobl, H. ; Lewis, A. R. One And Two-Dimensional Solid-State Nmr Investigations Of The Three-Dimensional Structures Of Zeolite-Organic Sorbate Complexes. In Zeolites: A Refined Tool for Designing Catalytic Sites; Bonneviot, L. ; Kaliaguine, S. ; Zeolites: A Refined Tool for Designing Catalytic Sites; Elsevier Science Publ B V: Amsterdam, 1995; Vol. 97, pp. 1-10.

1994

Fyfe, C. A. ; Niu, J. ; Rettig, S. J. ; Wang, D. W. ; Poliks, M. D. Nmr Investigations Of The Possible Cross-Reactions Between Cyanate And Epoxy-Resins. Journal of Polymer Science Part a-Polymer Chemistry 1994, 32, 2203-2221.
Fyfe, C. A. ; Wongmoon, K. C. ; Grondey, H. ; Mueller, K. T. Increased Efficiency Of Coherence Transfer In Cross-Polarization Nmr From Quadrupolar Nuclei - Dynamic-Angle Cross-Polarization. Journal of Physical Chemistry 1994, 98, 2139-2142.
Fox, C. A. ; Preston, C. M. ; Fyfe, C. A. Micromorphological And C-13 Nmr Characterization Of A Humic, Lignic, And Histic Folisol From British-Columbia. Canadian Journal of Soil Science 1994, 74, 1-15.
Fyfe, C. A. ; Mueller, K. T. ; Wongmoon, K. C. Cross-Polarization Processes Involving Less Common Pairs Of Nuclei. In Nuclear Magnetic Resonance in Modern Technology; Maciel, G. E. ; Nuclear Magnetic Resonance in Modern Technology; Kluwer Academic Publ: Dordrecht, 1994; Vol. 447, pp. 447-482.
Fyfe, C. A. ; Fu, G. Y. ; Grondey, H. Pillaring Of Layered Double Hydroxides With Cage-Like Polysilicates - A Possible New Class Of Base Catalysts Or Catalyst Precursors. In Better Ceramics through Chemistry Vi; Cheetham, A. K. ; Brinker, C. J. ; Mecartney, M. L. ; Sanchez, C. ; Better Ceramics through Chemistry Vi; Materials Research Soc: Pittsburgh, 1994; Vol. 346, pp. 907-913.
Fyfe, C. A. ; Kokotailo, G. T. Solid State Nmr Investigations Of Zeolites And Related Materials. In Nuclear Magnetic Resonance in Modern Technology; Maciel, G. E. ; Nuclear Magnetic Resonance in Modern Technology; Kluwer Academic Publ: Dordrecht, 1994; Vol. 447, pp. 277-337.

1993

Marler, B. ; Deroche, C. ; Gies, H. ; Fyfe, C. A. ; Grondey, H. ; Kokotailo, G. T. ; Feng, Y. ; Ernst, S. ; Weitkamp, J. ; Cox, D. E. The Structure Of Zeolite Zsm-23 (Mtt) Refined From Synchrotron X-Ray-Powder Data. Journal of Applied Crystallography 1993, 26, 636-644.
Niessner, N. ; Muhlebach, A. ; Lyerla, J. R. ; Facey, G. A. ; Fyfe, C. A. Synthesis Of Isotopically Labeled Monomers And Polymers Of 4-Hydroxybenzoic Acid And 6-Hydroxy-2-Naphthoic Acid. Makromolekulare Chemie-Macromolecular Chemistry and Physics 1993, 194, 649-663.
Fyfe, C. A. ; Mueller, K. T. ; Grondey, H. ; Wongmoon, K. C. Solid-State Double-Resonance Nmr Experiments Involving Quadrupolar And Spin 1/2 Nuclei. Journal of Physical Chemistry 1993, 97, 13484-13495.

1992

Fyfe, C. A. ; Mueller, K. T. ; Grondey, H. ; Wongmoon, K. C. Dipolar Dephasing Between Quadrupolar And Spin-1/2 Nuclei - Redor And Tedor Nmr Experiments On Vpi-5. Chemical Physics Letters 1992, 199, 198-204.
Fyfe, C. A. ; Fahie, B. J. ; Lyerla, J. R. ; Economy, J. ; Niessner, N. ; Muhlebach, A. ; Facey, G. A. Demonstration Of The Liquid-Crystalline Behavior Of A Rigid-Backbone Polyester In A Magnetic-Field. Macromolecules 1992, 25, 1623-1624.
Fyfe, C. A. ; Grondey, H. ; Mueller, K. T. ; Wongmoon, K. C. ; Markus, T. Coherence Transfer Involving Quadrupolar Nuclei In Solids - Al-27-Reversible-Arrow-P-31 Cross-Polarization Nmr In The Molecular-Sieve Vpi-5. Journal of the American Chemical Society 1992, 114, 5876-5878.
Fyfe, C. A. ; Grondey, H. ; Feng, Y. ; Kokotailo, G. T. ; Ernst, S. ; Weitkamp, J. 2-Dimensional Solid-State Si-29 Nmr Investigation Of The 3-Dimensional Bonding Connectivities And Structure Of Zeolite Zsm-23. Zeolites 1992, 12, 50-53.
Chivers, T. ; Edwards, M. ; Fyfe, C. A. ; Randall, L. H. Solid-State P-31 Nmr Investigations Of Unsaturated Phosphorus Nitrogen Sulfur Rings. Magnetic Resonance in Chemistry 1992, 30, 1220-1223.
Fyfe, C. A. ; Zhang, Y. ; Aroca, P. An Alternative Preparation Of Organofunctionalized Silica-Gels And Their Characterization By 2-Dimensional High-Resolution Solid-State Heteronuclear Nmr Correlation Spectroscopy. Journal of the American Chemical Society 1992, 114, 3252-3255.

1991

Fyfe, C. A. ; Feng, Y. ; Grondey, H. ; Kokotailo, G. T. ; Gies, H. One-Dimensional And 2-Dimensional High-Resolution Solid-State Nmr-Studies Of Zeolite Lattice Structures. Chemical Reviews 1991, 91, 1525-1543.
Fyfe, C. A. ; Feng, Y. ; Grondey, H. ; Kokotailo, G. T. ; Mar, A. Natural Abundance, 2-Dimensional Si-29 Mas Nmr Investigation Of The 3-Dimensional Bonding Connectivities In The High-Temperature And Low-Temperature Forms Of Zeolite Zsm-11. Journal of Physical Chemistry 1991, 95, 3747-3751.
Kokotailo, G. T. ; Fyfe, C. A. ; Feng, Y. ; Grondey, H. Characterization Of Zeolite-Cracking Catalysts. In Fluid Catalytic Cracking Ii - Concepts in Catalyst Design; Occelli, M. L. ; Fluid Catalytic Cracking Ii - Concepts in Catalyst Design; Amer Chemical Soc: Washington, 1991; Vol. 452, pp. 27-44.
Kokotailo, G. T. ; Fyfe, C. A. ; Feng, Y. ; Grondey, H. Characterization Of Zeolite-Cracking Catalysts. Acs Symposium Series 1991, 452, 27-44.
Gies, H. ; Marler, B. ; Fyfe, C. ; Kokotailo, G. ; Feng, Y. ; Cox, D. E. The Combination Of Synchrotron Powder Diffraction And High-Resolution Solid-State Nmr Experiments. Journal of Physics and Chemistry of Solids 1991, 52, 1235-1241.

1990

Fyfe, C. A. ; Feng, Y. ; Grondey, H. ; Kokotailo, G. T. Characterization Of A High-Loaded Intercalate Of Para-Xylene With A Highly Siliceous Form Of Zsm-5 By High-Resolution Si-29 Solid-State Nmr-Spectroscopy. Journal of the Chemical Society-Chemical Communications 1990, 1224-1226.
Fyfe, C. A. ; Grondey, H. ; Feng, Y. ; Kokotailo, G. T. Investigation Of The 3-Dimensional Si-O-Si Connectivities In The Monoclinic Form Of Zeolite Zsm-5 By 2-Dimensional Si-29 Inadequate Experiments. Chemical Physics Letters 1990, 173, 211-215.
Fyfe, C. A. ; Grondey, H. ; Feng, Y. ; Kokotailo, G. T. Natural-Abundance 2-Dimensional Si-29 Mas Nmr Investigation Of The 3-Dimensional Bonding Connectivities In The Zeolite Catalyst Zsm-5. Journal of the American Chemical Society 1990, 112, 8812-8820.
Fyfe, C. A. ; Gies, H. ; Kokotailo, G. T. ; Marler, B. ; Cox, D. E. Crystal-Structure Of Silica-Zsm-12 By The Combined Use Of High-Resolution Solid-State Mas Nmr-Spectroscopy And Synchrotron X-Ray-Powder Diffraction. Journal of Physical Chemistry 1990, 94, 3718-3721.
Fyfe, C. A. ; Gies, H. A Si-29 Nmr-Study Of Natural And Synthetic Melanophlogites, The Silica Analogs Of The Clathrate Hydrates Of Type-1. Journal of Inclusion Phenomena and Molecular Recognition in Chemistry 1990, 8, 235-239.
Fyfe, C. A. ; Gies, H. ; Feng, Y. ; Grondey, H. 2-Dimensional Si-29 Mas Nmr Investigation Of The 3-Dimensional Structure Of Zeolite Dd3R. Zeolites 1990, 10, 278-282.
Fyfe, C. A. ; Feng, Y. ; Gies, H. ; Grondey, H. ; Kokotailo, G. T. Natural-Abundance 2-Dimensional Solid-State Si-29 Nmr Investigations Of 3-Dimensional Lattice Connectivities In Zeolite Structures. Journal of the American Chemical Society 1990, 112, 3264-3270.
Lyerla, J. R. ; Economy, J. ; Maresch, G. G. ; Muhlebach, A. ; Yannoni, C. S. ; Fyfe, C. A. Molecular-Motion In The Homopolyester Of 4-Hydroxybenzoic Acid. Acs Symposium Series 1990, 435, 359-368.
Oehler, U. M. ; Janzen, E. G. ; Betteridge, K. ; Fyfe, C. ; Towner, R. A. ; Savage, N. ; Scodras, J. Investigations Of The Horse Conceptus Via Magnetic-Resonance-Imaging (Mri) And Nitroxide Spin Labels As Contrast Agents. Free Radical Research Communications 1990, 9, 391-397.

1989

Kokotailo, G. T. ; Fyfe, C. A. Zeolites - Unique Materials For Research And Industry. Journal of Physics and Chemistry of Solids 1989, 50, 441-447.
Fyfe, C. A. ; Gies, H. ; Feng, Y. 3-Dimensional Lattice Connectivities From Two-Dimensional High-Resolution Solid-State Nmr - Si-29 Mas Nmr Investigation Of The Silicate Lattice Of Zeolite Zsm-39 (Dodecasil-3C). Journal of the American Chemical Society 1989, 111, 7702-7707.
Fyfe, C. A. ; Gies, H. ; Feng, Y. Demonstration Of 3-Dimensional Lattice Connectivities In Zeolites By Two-Dimensional High-Resolution Solid-State Nmr-Spectroscopy. Journal of the Chemical Society-Chemical Communications 1989, 1240-1242.
Fyfe, C. A. ; Gies, H. ; Feng, Y. ; Kokotailo, G. T. Determination Of 3-Dimensional Lattice Connectivities In Zeolites Using Natural-Abundance Si-29 Two-Dimensional Nmr And The Direct Observation Of Si-29-O-Si-29 Couplings. Nature 1989, 341, 223-225.
Fyfe, C. A. ; Gies, H. ; Kokotailo, G. T. ; Pasztor, C. ; Strobl, H. ; Cox, D. E. Detailed Investigation Of The Lattice Structure Of Zeolite Zsm-11 By A Combination Of Solid-State Nmr And Synchrotron X-Ray-Diffraction Techniques. Journal of the American Chemical Society 1989, 111, 2470-2474.

1988

Fyfe, C. A. ; Strobl, H. ; Gies, H. ; Kokotailo, G. T. High-Resolution Solid-State Nmr Investigation Of The Nature Of The Interaction Between Organic Substrates And The Zeolite Zsm-5 Lattice. Canadian Journal of Chemistry-Revue Canadienne De Chimie 1988, 66, 1942-1947.
Fyfe, C. A. Mcdowell,charles,a. - Dedication. Canadian Journal of Chemistry-Revue Canadienne De Chimie 1988, 66, R3-R3.

1970

Fyfe, C. A. ; Gilson, D. F. R. ; Thompson, K. H. Molecular Motion In Solid Pyrene. Chemical Physics Letters 1970, 5, 215-217.

1968

Fyfe, C. A. ; McDowell, C. A. Molecular Motion Is Solid Tropylium Salts. Chemical Physics Letters 1968, 2, 170-172.