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STRUCTURAL STUDIES OF ORGANOBORON COMPOUNDS .62. SYNTHESIS AND STRUCTURE OF VARIOUS N-ALKYLATED 1,3-DIOXA-4-AZA-2-BORACYCLOHEXANES

TitleSTRUCTURAL STUDIES OF ORGANOBORON COMPOUNDS .62. SYNTHESIS AND STRUCTURE OF VARIOUS N-ALKYLATED 1,3-DIOXA-4-AZA-2-BORACYCLOHEXANES
Publication TypeJournal Article
Year of Publication1994
AuthorsKliegel, W, Amt, H, Becker, H, Lauterbach, U, Lubkowitz, G, Rettig, SJ, Trotter, J
JournalCanadian Journal of Chemistry-Revue Canadienne De Chimie
Volume72
Pagination2118-2130
Date PublishedOct
Type of ArticleArticle
ISBN Number0008-4042
KeywordsNITRONES, RING-CHAIN ISOMERISM
Abstract

{The synthesis of a number of variously substituted N-alkyl 2-hydroxyaminoalkanols 3 and their reactions with phenylboronic acid are detailed. The crystalline products proved to be 1:2 condensates 4 in a few cases and 1:1 condensates 5 in all the other cases studied. Crystals of 2-mesityl-6,6-pentamethylene-1,3-dioxa-4-aza-2-boracyclohexane, 5l, are triclinic

URL<Go to ISI>://A1994PP74000012