Research & Teaching Faculty

Plant polysaccharide itself as hydrogen bond donor in a deep eutectic system-based mechanochemical extraction method

TitlePlant polysaccharide itself as hydrogen bond donor in a deep eutectic system-based mechanochemical extraction method
Publication TypeJournal Article
Year of Publication2023
AuthorsLiu, M, Wang, S, Bi, W, Chen, DDY
JournalFood Chemistry
Volume399
Pagination133941
Date Published01/2023
Type of ArticleResearch
ISSN0308-8146
KeywordsDeep eutectic solvents (DES), Deep eutectic system (DESys), hydrogen bonds, Plant natural products, POLYSACCHARIDE
Abstract

A deep eutectic system (DESys) is formed when a hydrogen bond acceptor (HBA) is processed with polysaccharide (hydrogen bond donor, HBD) containing plant substance in water to dissolve, extract, and recover the polysaccharide directly, instead of using a traditional deep eutectic solvent (DES). The extraction efficiency is enhanced by the direct formation of the DESys, in a mechanochemical extraction (MCE) system. Key factors affecting the extraction efficiency were systematically studied and optimized. The effects of the DESys on the structure and physicochemical properties of polysaccharides were studied by several analytical techniques. The findings demonstrated that the direct DESys formation extraction efficiency was superior than that of traditional extraction methods while retaining physicochemical properties of polysaccharides. Moreover, the composition of polysaccharides extracted with this method is different from that obtained by conventional methods. The recovery and purification process of polysaccharides is simplified by eliminating the need for an additional HBD.

URLhttps://www.sciencedirect.com/science/article/pii/S0308814622019033
DOI10.1016/j.foodchem.2022.133941