Research & Faculty

Shared Instrument Facility (SIF)

About

The Shared Instrument Facility (SIF) is an interdisciplinary laboratory space featuring a number of state-of-the-art scientific instruments available for teaching (Chem 315, 325, 335, 345, 425, 445) and research.

 

Services:

Our primary focus is on providing services for the Chemistry Department; however we have the capability to service external academic and industry clients. Please contact the Lab Director for more information.

 

Contact(s):

Yurou Sang, Lab Director

Office: B352

Email:

Location: RM B353

- - - - - - - - - - - - - -

Dr. Emily Seo, Lab Director (on maternity leave)

Office: B352

Email:

Location: RM B353

 

The Shared Instrument Facility

Department of Chemistry

2036 Main Mall,

Vancouver, B.C.

Canada V6T 1Z1

Tel: (604) 822-1982

Fax: (604) 822-2847

Instruments

Atomic force microscope (AFM)

The Nanosurf EasyScan 2 AFM is a scanning microscope system, capable of performing nanometer-scale measurements in air. This AFM module can be used with both solid and liquid samples operated with static mode or dynamic mode.

AFM

Capillary Electrophoresis (CE)-Diode Array Detector (DAD)

The Agilent 7100 CE system with ChemStation Software provides HPLC-like sensitivity to a wide range of analytical challenges. This instrument offers the advantage that several separation modes can be run on a single instrument.

  • Highly sensitive
  • Flexible separation modes
  • Increased sensitivity with extended light path capillary

Circular dichroism/optical rotary dispersion spectrophotometer (CD/ORD)

The Jasco J-815 CD spectrophotometer is capable to measure the optical activity of chiral compounds from 163-1100 nm and has an air cooled Xenon arc lamp or water cooled Xenon lamp.

  • Sample type: solid or liquid samples
  • Measurement from 163 – 1100 nm
  • Operated with Spectra Manager software
Circular dichroism

Fluorescence Spectrophotometer

The Agilent Cary Eclipse Fluorescence Spectrophotometer is used to measure the emission of light from samples in four modes: fluorescence, phosphorescence or chemi/bio luminescence. The Xenon flash lamp is used for the instrument to provide superior sensitivity, high signal-to noise, and fast kinetics.

Fluorescence Spectrophotometer

Fourier Transfer-Infrared Spectroscopy (FT-IR) with attenuated total reflectance (ATR)

PerkinElmer Frontier FT-IR is used to obtain an infrared spectrum of absorption of a solid, liquid or gas. The FT-IR offers flexible system configurations in the near, near-mid, mid-far and far infrared regions, and support an extensive range of applications.      

  • Can be used to measure liquid, solid or gas samples
  • The user should bring their own gas cell while measuring gas samples
  • Characterize novel materials
  • Fast analysis time

Gas chromatograph (GC) with flame ionization detector (FID) and thermal conductivity detector (TCD)

The Bruker 450 GC includes a flame ionization detector (FID) operated with GalaxieTM software is used for identifying and quantifying volatile and semi-volatile compounds in a variety of samples. This instrument can utilize up to three injectors and detectors.

  • Good flexibility and performance to suit the widest range of application needs
  • Auto-sampler is available for multi-sampling

 

GC

Gas Chromatograph Mass Spectrometry (GC-MS)

Agilent 6890N GC coupled with 5975B MS detector is operated with ChemStation Software which high sensitivity analysis for gas phase samples.

  • Split-splitless injection system
  • Built in library is available for identifing unknown compounds
  • Auto-sampler is available for multisampling

 

GCMS

Ultra Higher Performance Liquid Chromatography (uHPLC)-Diode Array Detector (DAD)

The Agilent 1260 Infinity Binary uHPLC system enables to handle 600 bar pressure while retaining the practicality and principles of HPLC, a separation/isolation technique.

  • Only manual injector available
  • Fixed injection volume (5uL)
uHPLC

Ultra Higher Performance Liquid Chromatography (uHPLC)-Mass Spectrometer (MS)

The Agilent Quadruple uHPLC-MS system combines the physical separation capabilities of uHPLC with the mass analysis capabilities of mass spectrometry. It is a powerful technique with very high sensitivity and selectivity.

  • Auto-sampler available for multi-sampling
  • Low sample volume (<0.5mL)
  • Operated with ChemStation

 

LCMS

Nuclear Magnetic Resonance (NMR) Spectrometer

Bruker Avance-III 300 NMR is a state-of-the-art NMR spectrometer is operating at 300mHz for 1H and 13C observation. This instrument is fully capable of performing any 1D or 2D NMR experiment possible on a 2-channel NMR spectrometer.  

  • Only accept drop in appointment for departmental users
  • For external users, please contact the NMR Facility for measuring or submitting NMR samples

For high resolution NMR spectroscopy, please contact the High-Resolution NMR Analytical Services and Research Support Facility.

 

Nuclear Magnetic Resonance

Polarimeter

Jasco P-2000 polarimeter can be used to measure the angel of rotation caused by passing polarized light through an optically active substance. It has analytical wavelengths from UV-Vis to NIR.

  • Sample capacity: 8.5-8.7mL
Polarimeter

Stopped Flow Instrument

The stopped flow instrument is a rapid mixing device used to study the chemical kinetics of a reaction in solution

Stopped Flow Instrument

Lambda 25 UV/Uis Spectrophotometer

Lambda 25 is used for routine UV/Vis applications, pharmacopoeia and regulatory tests and liquids analysis. The comprehensive range of operating modes provides trustworthy results for a range of analysis including quantitative measurements and kinetics studies.

  • Range: 190-1100 nm
  • Bandwidth: 1nm (fixed)
  • Modes of Operation: scanning, wavelength program, time-drive, rate, quant, scanning quant
  • Double-beam operation
  • High throughput, low stray-light optics
  • Pre-aligned deuterium and tungsten-halogen lamps
  • Operated with UV WinLab Software
Lambda 25 UV/Uis

UV/Vis spectrophotometer

The UV-Vis-NIR spectrophotometer detects in the 175-3300 nm range and can extend its near infrared (NIR) range to 3300 nm.

UV/Vis spectrophotometer

Fisher Scientific UV-Vis

The Helios Zsta UV-Vis spectrophotometer can be used for routine research applications.

Fisher Scientific UV-Vis

Services

Our primary focus is on providing services for the Chemistry Department; however we have the capability to service external academic and industry clients. Please contact the Lab Director for more information.

Training

Prior to work, all users have to complete BOTH instrument-specific and Chemical Safety Training — no exceptions. Please call or e-mail to arrange a time with us for training on the listed instruments,

  • Atomic force microscope (AFM)
  • Capillary electrophoresis chromatograph (CE)
  • Circular dichroism/optical rotary dispersion spectrophotometer (CD/ORD)
  • Fluorometer
  • Fourier transform infrared spectrometer (FTIR) with attenuated total reflectance (ATR)
  • Gas chromatograph (GC) with flame ionization detector (FID) and thermal conductivity detector (TCD)
  • Gas chromatograph-mass spectrometer (GC-MS)
  • Liquid chromatograph-mass spectrometer (LC-MS)
  • Nuclear magnetic resonance spectrometer (NMR)
  • Polarimeter
  • Stopped-flow instrument
  • Ultra-high-performance liquid chromatograph (uHPLC)
  • Three UV/Vis spectrophotometers - one with NIR capabilities
  • Spectrometer

For Chemical Safety training, please contact the department Safety Program Administrator

Helen Wright

Office: Chemistry A237

Phone (office): (604) 827-5216

Email: 

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SIF Instrument Booking System

All users need to reserve the instruments through the instrument booking site https://wapps.chem.ubc.ca/sif or contact the Lab Director.

 

SIF Instrument Usage Cost

Contact the Lab Director for the fee schedule.

 

General Rules for Working in the Shared Instrument Facility

  • Booking is done through the online system, except for NMR (drop-in service);
  • Do not bring any biohazardous, radioactive or toxic materials;
  • Bench surfaces must be left clear of glassware, garbage and spills;
  • Waste must be decontaminated and disposed of;
  • If the gas cylinder pressure is under 500 psi, please bring up a new one and write it in the logbook or ask SIF technician to replace it for you. Do not leave gas cylinders completely empty.
  • Removing their work materials from workstations as tasks are completed
  • Sign the log book for all the SIF instruments after use;
  • Login/logout from Windows will keep track of time spend on the instrument (billing), therefore remember to logout.

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